Chem. J. Chinese Universities ›› 2014, Vol. 35 ›› Issue (2): 250.doi: 10.7503/cjcu20130801
• Analytical Chemistry • Previous Articles Next Articles
YUE Weichao, CAI Zhuo*(), JIANG Cuiwen, YE Danni
Received:
2013-08-19
Online:
2014-02-10
Published:
2013-12-05
Contact:
CAI Zhuo
E-mail:zhuocai@gxu.edu.cn
Supported by:
CLC Number:
TrendMD:
YUE Weichao, CAI Zhuo, JIANG Cuiwen, YE Danni. Determination of Levodopa Using Biosynthesed Gold Nanoparticles/Multiwalled Carbon Nanotubes/L-Cysteine Composite Film Modified Glassy Carbon Electrode†[J]. Chem. J. Chinese Universities, 2014, 35(2): 250.
Fig.4 Alterating current impedance spectra of GCE(a), MWCNTs/GCE(b) MWCNTs/L-Cys/GCE(c) and Au/MWCNTs/L-Cys/GCE(d) in 0.10 mol/L KCl containing 5.0×10-3 mol/L Fe(CN)63-/4-(volume ratio 1∶1)Frequency range: 0.001—105 Hz.
Fig.6 CV curves of 1.0×10-4 mol/L levodopa in buffers with different pH valuespH values from a to g: 2.6, 3.0, 4.0, 5.0, 6.0, 7.0, 8.0. Inset shows the effect of pH on peak potential.
Fig.7 Cyclic voltammograms of 1.0×10-4 mol/L levodopa with different scan rates(A), effects of the natural logarithm of scan rate on peak potential(B) and the square root of scan rate on peak current(C)Scan rate(mV·s-1) from a to i: 30, 60, 90, 120, 150, 180, 210, 240, 270.
Fig.8 Differential pulse voltammograms of levodopa with different concentrations(A) and calibration curves of levodopa in the range of 0.6—40 μmol/L(B) and 60—120 μmol/L(C)(A) c(Levodopa)/(μmol·L-1): 0.6, 0.8, 2, 4, 6, 8, 20, 40, 60, 80, 100, 120.
Labelled amount/(mg·table-1) | Found/(mg·table-1) | |
---|---|---|
Electrochemical method | UV-Vis method | |
250.0 | 252.3 | 256.3 |
250.0 | 249.4 | 254.5 |
250.0 | 251.6 | 253.2 |
250.0 | 248.5 | 255.6 |
250.0 | 250.5 | 253.2 |
Average value±SD | 250.5±1.4 | 254.9±2.1 |
Table 1 Determination of levodopa in tablet
Labelled amount/(mg·table-1) | Found/(mg·table-1) | |
---|---|---|
Electrochemical method | UV-Vis method | |
250.0 | 252.3 | 256.3 |
250.0 | 249.4 | 254.5 |
250.0 | 251.6 | 253.2 |
250.0 | 248.5 | 255.6 |
250.0 | 250.5 | 253.2 |
Average value±SD | 250.5±1.4 | 254.9±2.1 |
Labelled amount/(μmol·L-1) | Added/(μmol·L-1) | Found/(μmol·L-1) | Recovery(%) | RSD(%) |
---|---|---|---|---|
2.02 | 2.00 | 3.99 | 99.2 | 4.04 |
2.02 | 4.00 | 6.10 | 101.3 | |
2.02 | 6.00 | 8.22 | 91.2 | |
2.02 | 8.00 | 10.05 | 102.5 | |
2.02 | 10.00 | 12.06 | 100.3 |
Table 2 Recovery of the method
Labelled amount/(μmol·L-1) | Added/(μmol·L-1) | Found/(μmol·L-1) | Recovery(%) | RSD(%) |
---|---|---|---|---|
2.02 | 2.00 | 3.99 | 99.2 | 4.04 |
2.02 | 4.00 | 6.10 | 101.3 | |
2.02 | 6.00 | 8.22 | 91.2 | |
2.02 | 8.00 | 10.05 | 102.5 | |
2.02 | 10.00 | 12.06 | 100.3 |
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