微波辅助提取-气相色谱质谱联用测定肉桂中的挥发油

高等学校化学学报 ›› 2009, Vol. 30 ›› Issue (7): 1300.

微波辅助提取-气相色谱质谱联用测定肉桂中的挥发油

朱晓楠¹, 魏士刚¹, 王浩南², 孙颖¹, 姜春竹¹, 王健¹, 王璐¹, 王丽英¹, 宋大千¹

1. 吉林大学化学学院,
2. 环境与资源学院, 长春 130012

收稿日期:2009-01-13 出版日期:2009-07-10 发布日期:2009-07-10
通讯作者: 宋大千, 男, 博士, 教授, 博士生导师, 主要从事生物分析和药物分析研究. E-mail: songdq@jlu.edu.cn

Analysis of Essential Oil from Cinnamomum cassia Presl by Microwave-assisted Extraction Coupled with Gas Chromatography-Mass Spectrometry

ZHU Xiao-Nan¹, WEI Shi-Gang¹, WANG Hao-Nan², SUN Ying¹, JIANG Chun-Zhu¹, WANG Jian¹, WANG Lu¹, WANG Li-Ying¹, SONG Da-Qian^1*

1. College of Chemistry,
2. College of Environment and Resource, Jilin University, Changchun 130012, China

Received:2009-01-13 Online:2009-07-10 Published:2009-07-10
Contact: SONG Da-Qian. E-mail: songdq@jlu.edu.cn

摘要/Abstract

摘要：

利用非极性溶剂微波辅助提取(NPSMAE)-气相色谱质谱联用研究了肉桂中的挥发油成分, 并测定了挥发油中的主要成分肉桂醛(Cinnamaldehyde)的含量. 考察了NPSMAE提取溶剂的种类、提取温度、提取时间及固液比等对测定的影响, 同时将NPSMAE与超声波辅助提取(UAE)及水蒸气蒸馏(HD)等方法进行了比较. 结果表明, 与常规提取方法相比, NPSMAE具有提取时间短、提取产率高等优点, 是一种实用的中药挥发油提取方法.

关键词: 肉桂; 挥发油; 非极性溶剂微波辅助提取; 气相色谱质谱联用

Abstract:

The essential oil from Cinnamomum cassia Presl was studied by non-polar solvent microwave-assisted extraction(NPSMAE) coupled with gas chromatagraphy-mass spectrometry(GC-MS). The cinnamaldehyde as a main component in the essential oil was determined. The effects of type of solvent, temperature, extraction time and ratio of solid to solvent(m/V) were examined and optimized. Compared with UAE and HD, NPSMAE has several advantages such as shorter extraction time and higher extraction yield. The proposed method is suitable for the extraction of essential oil.

Key words: Cinnamomum cassia Presl; Essential oil; Non-polar solvent microwave-assisted extraction; Gas chromatagraphy-mass spectrometry

TrendMD:

朱晓楠, 魏士刚, 王浩南, 孙颖, 姜春竹, 王健, 王璐, 王丽英, 宋大千. 微波辅助提取-气相色谱质谱联用测定肉桂中的挥发油. 高等学校化学学报, 2009, 30(7): 1300.

ZHU Xiao-Nan, WEI Shi-Gang, WANG Hao-Nan, SUN Ying, JIANG Chun-Zhu, ....... Analysis of Essential Oil from Cinnamomum cassia Presl by Microwave-assisted Extraction Coupled with Gas Chromatography-Mass Spectrometry. Chem. J. Chinese Universities, 2009, 30(7): 1300.

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