高等学校化学学报

高等学校化学学报 ›› 2005, Vol. 26 ›› Issue (9): 1618.

• 研究论文 • 上一篇    下一篇

微波萃取高效液相色谱法测定口红中芳香胺类化合物

汪子明1, 周新1, 郑健1, 张寒琦1, 刘丽2, 李英2, 刘志红2, 王宏菊2, 曾红2, 何慧2   

  1. 1. 吉林大学化学学院,长春130012;
    2. 深圳出入境检验检疫局,深圳518045
  • 收稿日期:2004-11-01 出版日期:2005-09-10 发布日期:2005-09-10

Determination of Aromatic Amine Compounds in Lipstick by Microwave-assisted Extraction High Performance Liquid Chromatography

WANG Zi-Ming1, ZHOU Xin1, ZHENG Jian1, ZHANG Han-Qi1, LIU Li2, LI Ying2, LIU Zhi-Hong2, WANG Hong-Ju2, ZENG Hong2, HE Hui2   

  1. 1. College of Chemistry, Jilin University, Changchun 130012, China;
    2. Shenzhen Entry-exit Inspection and Quarantine Bureau, Shenzhen 518045, China
  • Received:2004-11-01 Online:2005-09-10 Published:2005-09-10

PDF (PC)

被引次数

50

摘要： 利用微波萃取高效液相色谱法测定了口红中芳香胺类化合物.先将口红涂于玻璃片上,然后用微波萃取和高效液相色谱法测定萃取液中的芳香胺类化合物.研究了3种市售口红并得到了芳香胺类化合物的定量测定结果.考察了微波萃取的条件,并将薄层色谱等萃取分离方法和微波萃取法进行了比较,证明微波萃取法在萃取膏状物和蜡状物中的组分时,具有比其它方法更加方便、快速等优点.

关键词: 微波萃取, 口红, 芳香胺

Abstract: A new method, microwave-assisted extraction(MAE) high-performance liquid chromatography(HPLC), for quantitative determination of aromatic amine compounds in lipstick was developed. The lipstick sample was coated on glass slide, then the glass was put in the extraction vessel and aromatic amine compounds in the sample were extracted by microwave radiation. The obtained extract was analyzed by HPLC. Three commercial lipsticks were analyzed and the satisfactory results were obtained. Compared with the other extraction methods, the MAE takes shorter time and the extraction yields of the aromatic amine compounds obtained by using MAE are higher.

Key words: Microwave-assisted extraction, Lipstick, Aromatic amine

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