高等学校化学学报 ›› 2003, Vol. 24 ›› Issue (4): 621.

• 研究简报 • 上一篇    下一篇

高分辨率电喷雾飞行时间质谱测定丹参脂溶性组分

于文佳, 何坚, 沈金灿, 王小如   

  1. 厦门大学现代分析科学教育部重点实验室, 厦门 361005
  • 收稿日期:2002-05-15 出版日期:2003-04-24 发布日期:2003-04-24
  • 通讯作者: 王小如(1949年出生),女,教授,博士生导师,从事原子光谱、质谱及中药材GAP研究.E-mail:xE-mairwE-maiang@xmE-maiu.edu.cn E-mail:xE-mairwE-maiang@xmE-maiu.edu.cn
  • 基金资助:

    国家自然科学专项基金(批准号:H-29927002);国家自然科学重点基金(批准号:29245110);香港特区政府创新科技署;科技部中药现代化重中之重“九五”项目资助

Determination of Fat soluble Components in Danshen by High-ResolutionElectrospray Ionization Time-of-flight Mass Spectrometry

YU Wen Jia, HE Jian, SHEN Jin Can, WANG Xiao Ru   

  1. The Key Laboratory of Analytical Science of MOE, Xiamen University, Xiamen 361005, China
  • Received:2002-05-15 Online:2003-04-24 Published:2003-04-24

关键词: 高分辨率电喷雾飞行时间质谱, 丹参, HPLC-ESI-MS, 中药指纹图谱

Abstract: An excellent analytical tool for the separation and analysis of TCM(Traditional Chinese Medicine) by using HR ESI TOF MS(High Resolution Electrospray Ionization Time of flight Mass Spectrometry) was developed. A home built HR ESI TOF MS was applied to detect fat soluble components in Danshen(Salvia miltiorrhiza Bage) directly. Compared with the method of HPLC ESI MS(High Performance Liquid Chromatograph Electrospray ionization Mass Spectrometry) method, HR ESI TOF MS method is more accurate, quick, simple and reliable, so the method can become an effective tool for the quality control of TCM.

Key words: High resolution electrospray ionization time of flight mass spectrometry, Danshen, HPLC ESI MS, TCM(Traditional Chinese Medicine) fingerprint

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