高等学校化学学报 ›› 2000, Vol. 21 ›› Issue (10): 1589.

• 论文 • 上一篇    下一篇

Solvothermal Preparation of Mn3O4 Nanoparticles and Effect of Temperature on Particle Size

SONG Rui1,2, WANG Hong-jun3, FENG Shou-hua 1   

  1. 1. 扬州大学理学院化学系, 扬州 225002;
    2. 总后重庆后勤工程学院化学部, 重庆 630042
  • 出版日期:2000-10-24 发布日期:2000-10-24
  • 通讯作者: 郭荣(1954年出生),男,博士、教授.主要从事胶体与界面科学及其相关领域的研究.
  • 基金资助:

    国家自然科学基金(批准号:29733130)资助

Solvothermal Preparation of Mn3O4 Nanoparticles and Effect of Temperature on Particle Size

SONG Rui1,2, WANG Hong-jun3, FENG Shou-hua 1   

  1. 1. Chemistry Department, Yangzhou University, Yangzhou 225002, China;
    2. Chemistry Division, Logistical Engineering University, Chongqing 400016, China
  • Online:2000-10-24 Published:2000-10-24

摘要: 将十六烷增溶于油酸钠/水体系层状液晶的油层,共聚单体4-烯丙基-4-羟基-1,6-庚二烯增溶于油酸钠/水体系层状液晶的两亲层,在同一两亲层内进行共聚反应,得到了具有层状结构、并具有较好表面活性的共聚物.

关键词: Solvothermal preparation, Mn3O4, Nanoparticle, Particle size

Abstract: In the lamellar liquid crystal(LLC) phase of NaOL/hexadecane/AHD-ol/H2Osystem, the small X-ray diffraction measurements show that hexadecane was solubilized in the oil layer, while AHD-ol, commoner in the amphiphile layer. Copolymerization of the double bonds in the middle hydrocarbon chain of NaOLand in the three double bonds of ADH-ol took place in each amphiphile layer of LLCphase. The polymer with LLCstructure and surface activity was obtained at 72 ℃.

Key words: Solvothermal preparation, Mn3O4, Nanoparticle, Particle size

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