高等学校化学学报

高等学校化学学报 ›› 1999, Vol. 20 ›› Issue (S1): 84.

• Atomic Spectrometry • 上一篇    下一篇

The Determination of Lead in Gasoline By a Hyphenation Technology of Microwave Extraction and AAS

SUN Xiao-Juan, ZHANG Zhi-Hong, Gan-Xue   

  1. Department of Applied Chemistry, Jiangsu Institute of Petrochemical Technology, Changzhou, Jiangsu 213016, P. R. China
  • 出版日期:1999-12-31 发布日期:1999-12-31

The Determination of Lead in Gasoline By a Hyphenation Technology of Microwave Extraction and AAS

SUN Xiao-Juan, ZHANG Zhi-Hong, Gan-Xue   

  1. Department of Applied Chemistry, Jiangsu Institute of Petrochemical Technology, Changzhou, Jiangsu 213016, P. R. China
  • Online:1999-12-31 Published:1999-12-31

PDF (PC)

被引次数

22

摘要：

Usually, for the determination of trace concentration of lead in gasoline, a routine sample pre-treatment procedure (such as iodine monochloride method or boiled hydrochloric extraction method) is coupled with a spectrometric detector, because tetraethyl lead and tetramethyl lead were added in gasoline as a antiknock component. These methods involved, however, are often complex, time-consuming, labor-intensive and,hence, susceptible to errors and pollution. Use of microwave energy enhance extraction of organic compounds from solid matrices was reported, but, enhance extraction of organic compounds from organic matrices (in especial from the gasoline), then turning the extraction substance into an inorganic compound was not reported.

Abstract:

Usually, for the determination of trace concentration of lead in gasoline, a routine sample pre-treatment procedure (such as iodine monochloride method or boiled hydrochloric extraction method) is coupled with a spectrometric detector, because tetraethyl lead and tetramethyl lead were added in gasoline as a antiknock component. These methods involved, however, are often complex, time-consuming, labor-intensive and,hence, susceptible to errors and pollution. Use of microwave energy enhance extraction of organic compounds from solid matrices was reported, but, enhance extraction of organic compounds from organic matrices (in especial from the gasoline), then turning the extraction substance into an inorganic compound was not reported.

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