高等学校化学学报

高等学校化学学报 ›› 1999, Vol. 20 ›› Issue (S1): 209.

• Chromatography and Separation Sciences • 上一篇    下一篇

Mechanistic Evaluation of the Resolution of Racemic N-Acyl-1-arylaminoalkanes on (-Acidic Chiral Stationary Phases

Jae Jeong Ryoo, Sung Hyun Im, Kwang-Pill Lee   

  1. Department of Chemistry, Graduate School, Kyungpook National University, Taegu, 702-701, Korea
  • 出版日期:1999-12-31 发布日期:1999-12-31

Mechanistic Evaluation of the Resolution of Racemic N-Acyl-1-arylaminoalkanes on (-Acidic Chiral Stationary Phases

Jae Jeong Ryoo, Sung Hyun Im, Kwang-Pill Lee   

  1. Department of Chemistry, Graduate School, Kyungpook National University, Taegu, 702-701, Korea
  • Online:1999-12-31 Published:1999-12-31

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被引次数

75

摘要：

Evaluation of a chiral separation mechanism of a racemic compound is very important to the development of more efficient CSP for a better resolution of the racemic compound. Racemic N-acyl-1-arylaminoalkanes were resolved on the three different Pirkle type (-acidic chiral stationary phases(CSPs), phenylglycine DNB CSP(CSP 1),norephedrine DNB CSP(CSP 2), and phenylglycinol DNB CSP(CSP 3).

Abstract:

Evaluation of a chiral separation mechanism of a racemic compound is very important to the development of more efficient CSP for a better resolution of the racemic compound. Racemic N-acyl-1-arylaminoalkanes were resolved on the three different Pirkle type (-acidic chiral stationary phases(CSPs), phenylglycine DNB CSP(CSP 1),norephedrine DNB CSP(CSP 2), and phenylglycinol DNB CSP(CSP 3).

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