高等学校化学学报

高等学校化学学报 ›› 1992, Vol. 13 ›› Issue (7): 932.

• 论文 • 上一篇    下一篇

N-烃氧丙酰基四氢噻唑-2-硫酮的合成

黄化民, 焦玉国, 李叶芝, 张所波, 张德胜   

  1. 吉林大学化学系, 长春, 130021
  • 收稿日期:1991-04-22 修回日期:1992-05-20 出版日期:1992-07-24 发布日期:1992-07-24
  • 通讯作者: 黄化民

Synthesis of N-Alkoxypropionyl-1,3-thiazolidine-2-thiones

HUANG Hua-min, JIAO Yu-guo, LI Ye-zhi, ZHANG Suo-bo, ZHANG De-sheng   

  1. Department of Chemistry, Jilin University, Changchun, 130023
  • Received:1991-04-22 Revised:1992-05-20 Online:1992-07-24 Published:1992-07-24

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被引次数

4

摘要： 在三聚氯氰存在下由烃氧丙酸与四氢噻唑-2-硫酮反应得到N-烃氧丙酰四氢噻哇-2-硫酮(2a-i),由2a,c-h与格氏试剂反应得到烃氧乙基苯基酮(3a,c-h).产物2a-i未见报道.

关键词: N-烃氧丙酰四氢噻唑-2-硫嗣, 烃氧乙基苯基酮, 三聚氯氰

Abstract: 3-Alkoxypropionyl-l,3-thiazolidine-2-thiones 2a-i were synthesized from 3-alkoxy-propionic acid and 1, 3-thiazolidine-2-thione by using cyanuric chloride as the condensing agent.Alkoxyethylphenyl ketones 3a,c-h were obtained by treatment of 2a,c-h with phenylmagnesium bromide 2a-i are new compounds.

Key words: N-3-Alkoxypropionyl-1,3-thiazolidine-2-thione, Alkoxyethyl phenyl ketone, Cyanuric chloride

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