高等学校化学学报

高等学校化学学报 ›› 1988, Vol. 9 ›› Issue (11): 1104.

• 论文 • 上一篇    下一篇

Er(PMAP)3·2H2O的合成及其晶体结构和分子结构

陈伯涛1, 任丽萍1, 罗保生2, 谌了容2   

  1. 1. 北京师范大学化学系;
    2. 武汉大学分析测试中心
  • 收稿日期:1987-05-30 出版日期:1988-11-24 发布日期:1988-11-24
  • 通讯作者: 陈伯涛

The Synthesis and Crystal, Molecular Structure of Er(PMAP)3·2H2O

Chen Botao1, Ren Liping1, Luo Baosheng2, Zhan Liaorong2   

  1. 1. Department of Chemistry, Bering Normal University, Beijing;
    2. The Analysis and Testing Centre, Wuhan Univesity, Wuhan
  • Received:1987-05-30 Online:1988-11-24 Published:1988-11-24

PDF (PC)

摘要： Er(PMAP)9·2H2O(PMAP=1-苯基-3-甲基-4-乙酰吡咯啉酮-5)属单斜晶系。空间群为P21/c,晶胞参数α=17,582(4)Å,b=12.346(2)Å,c=18.236(3)Å,β=102.8(2)°,Z=4,R=0.06298。

关键词: Er(PMAP)3·, 2H2O, 晶胞参数, 单斜晶系

Abstract: Er(PMAP)3·2H2O crystal belongs to monoclinic system. α=17.582 (4)Å, b= 12.346(2)Å,c = 18.236(3)Å, β=102.8(2)°. Space group P21/c, Z=4. The diffraction data(Mo, Kα) were collected with type CAD4(Holland) fpurcircle diffractomer. The structure was determined by heavy atom method and refined by least square program, R = 0.06298

Key words: Er(PMAP)3·2H2O, Cell parameters, Monoclinic system

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