高等学校化学学报 ›› 1986, Vol. 7 ›› Issue (8): 721.

• 研究论文 • 上一篇    下一篇

反式-二硝基-二苯并-18-冠醚-6的合成及结构测定

张惠祥, 孙允秀, 杨光第, 申成, 金长春   

  1. 吉林大学化学系
  • 收稿日期:1985-04-24 出版日期:1986-08-24 发布日期:1986-08-24

Synthesis and Structure Determination of Trans-Dinitro-Dibenzo-Eighteen-Crown-Six

Zhang Huixiang, Sun Yunxiu, Yang Guangdi, Shen Cheng, Jin Changchun   

  1. Department of Chemistry, Jilin University, Changchun
  • Received:1985-04-24 Online:1986-08-24 Published:1986-08-24

摘要: 本文对二苯并-18-冠醚-6进行硝化,然后将产物与钾盐反应,生成了二硝基-二苯并-18-冠醚-6-硫氰化钾一水络合物。用元素分析、红外光谱及X光衍射法测定了结构。

Abstract: In this paper,the dibenzo-eightecn-crown-six was nitrated,and the product obtained reacts with potassium solt to form the dinitro-dibenzo-eighteen-crown-six-potassum thiocynate-water complex.Its structure was determined with the elementary analysis,the infrared spectrum and X-ray diffraction method.

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