高等学校化学学报 ›› 1986, Vol. 7 ›› Issue (10): 909.
• 研究简报 • 上一篇 下一篇
胡秉方, 胡宗华
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Hu Bingfang, Hu Zunghua
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摘要： 作者为了获得O,O-(2,2′-联苯基)二硫代磷酸酯及具有醌基的二硫代磷酸酯供试验其杀虫、杀菌活性之用,合成了上述两类新化合物共十六个。今将合成反应,操作手续及有关这些化合物的数值简报如下。应用五硫化二磷和羟基化合物按文献一般方法制得了O,O-(2,2′-联苯基)二硫代磷酸及其酯十一个。
Abstract: Eight O,O-(2,2'-biphenyl)dithiophosphates were prepared successfully by the following reaction:Six tetra(O,O-dialkyi dithiophosphoryl)p-benzoquinone were prepared by the following reaction.The steric hindrance of t-butyl derivatives was considered to be responsible for the unsuccessfukness in proceeding the reaction.
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胡秉方, 胡宗华. O,O-(2,2'联苯基)二硫代磷酸酯及四(O,O-二烷基二硫代磷酰基)对-苯醌的合成. 高等学校化学学报, 1986, 7(10): 909.
Hu Bingfang, Hu Zunghua . The Synthesis of O,O-(2,2'-Biphenyldithiophosphates and Tetra-(O,O-Dialkyldithiophosphoryl )-p Benzoquinones. Chem. J. Chinese Universities, 1986, 7(10): 909.
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