高等学校化学学报 ›› 1984, Vol. 5 ›› Issue (4): 460.

• 研究简报 • 上一篇    下一篇

Ce(ph3PO)(DBM)2(NO3)2的合成与鉴定

朱文祥, 王德英, 陈伯涛, 金林培   

  1. 北京师范大学化学系
  • 收稿日期:1983-01-18 出版日期:1984-10-24 发布日期:1984-10-24

Synthesis and Characterization of Mixed-Ligand Complex Ce(ph3PO)(DBM)3(NO3)2

Zhu Wenxiang, Wang Deying, Chen Botao, Jin Linpei   

  1. Deptnent of Chemistry, Beijing Normal University, Beijing
  • Received:1983-01-18 Online:1984-10-24 Published:1984-10-24

摘要: β-二酮络合物已获得广泛而深入的研究,Ce(Ⅳ)的β-二酮类络合物的研究也有报导[1-3].但是,关于Ce(Ⅳ)的β-二酮与其它混合配体络合物的研究至今未见报导.我们以(NH4)2Ce(NO3)6为起始物质,经由双-(三苯基氧化膦)硝酸铈(Ⅳ)中间络合物在混合溶剂中与DBM反应制得该化合物.通过紫外、红外光谱以及1HNMR谱等研究,对该络合物的性质进行了讨论.

Abstract: Amixed-ligand complex was prepared via intermediate complex Ce(ph3PO)2(NO3)4 from a mixed-solvent of acetone and ethanol.Elemental analysis shows its formula to be Ce(ph3PO)(DBM)3(NO3)2. And its properties has also been studied by means of conductivity, IR, UVand 1H NMRtechniques.

TrendMD: