高等学校化学学报 ›› 2021, Vol. 42 ›› Issue (4): 1156.doi: 10.7503/cjcu20200506
收稿日期:
2020-07-31
出版日期:
2021-04-10
发布日期:
2020-11-10
通讯作者:
吕男
E-mail:luenan@jlu.edu.cn
基金资助:
DOU Shuzhen, WANG Zhongshun, LYU Nan()
Received:
2020-07-31
Online:
2021-04-10
Published:
2020-11-10
Contact:
LYU Nan
E-mail:luenan@jlu.edu.cn
Supported by:
摘要:
本文总结了多种构筑硅纳米结构的方法, 综述了近年来利用硅纳米结构提高表面辅助激光解吸/电离质谱(SALDI-MS)性能的研究工作, 展望了利用功能化的硅纳米结构表面进一步提高激光解吸/电离(LDI)效率的前景.
中图分类号:
TrendMD:
窦树珍, 王中舜, 吕男. 硅纳米结构对表面辅助激光解吸/电离质谱检测性能的提高. 高等学校化学学报, 2021, 42(4): 1156.
DOU Shuzhen, WANG Zhongshun, LYU Nan. Improving the Detection Performance of Surface-assisted Laser Desorption/ionization Mass Spectrometry by Silicon Nanostructures. Chem. J. Chinese Universities, 2021, 42(4): 1156.
Fig.1 Preparation of polymer ordered structure templates on silicon surface by photolithography(A), nano-imprinting lithography(B) and self-assembly colloidal sphere technology(C), transferring ordered structure from polymer template to silicon by reactive ion etching and metal-assisted chemical etching(D)
Fig.2 SEM of porous silicon in the top view(A) and the cross-sectional view(B), distinguishing smoker and non-smoker by comparison detection of nicotine from the MS finger imaging(C)[23] and the average S/N by breath samples(D)[24], Liquid-phase microextraction of analytes from complex samples on super-wetting porous silicon then LDI(E)[28](A—C) Copyright 2015, the Royal Society of Chemistry; (D) Copyright 2017, the Royal Society of Chemistry; (E) Copyright 2019, Elsevier.
Fig.3 Schematic diagram of selectivity of NIMS surface morphology(pore sizes) to molecule size(A) and the correlation of NIMS surface morphology(pore sizes) and molecular length regarding NIMS sensitivity(B)[30], NIMS based on the black silicon surface(C) and the sensitivity study of NIMS(D)[31], the physical and chemical properties of DIOS and NIMS surfaces and their limit of detection (LOD) (E)[33](A, B) Copyright 2017, American Chemical Society; (C, D) Copyright 2016, American Chemical Society; (E) Copyright 2020, American Chemical Society.
Fig.4 SEM of silicon nanowire in the top view(A) and the cross-sectional view(B)[36], comparison of the laser energy required on the silicon nanowire and porous silicon(C)[35], SALDI-MS spectrum for fresh and activated silicon nanowire(D)[36], schematic diagram of silicon nanowire tip enhanced electron transfer(E), extraction(F) and SALDI-MS detection thiabendazole by tip-contact sampling method(G)[37], microbial MS imaging on silicon nanowire of Aspergillus strains 3G and 3Y(H)[38](A, B, D) Copyright 2016, The Royal Society of Chemistry; (C) Copyright 2005, American Chemical Society; (E—G) Copyright 2018, American Chemical Society; (H) Copyright 2018, American Chemical Society and American Society of Pharmacognosy.
Fig.5 Optical image(a, g) and MS imaging of mouse brain tissue section on silicon nanopost array[from negative?ion spectra(b—f) , from positive?ion spectra(h—l)](A)[40], numbers of metabolites in silicon nanopost array and MALDI?MS analyses of hepatocyte extracts and urine sample(B)[44], SEM of silicon nanopost array and the correlation between the SALDI?MS signal intensity and the absorbance of silicon nanopost array(C)[45](A) Copyright 2016, Wiley-VCH; (B) Copyright 2019, American Chemical Society; (C) Copyright 2020, American Chemical Society.
Fig.6 Schematic illustration of the fabrication of silicon nanocone array as SALDI?MS substrate(A) and the dependence of S/N on the height of cones(B)[46], schematic illustration of the fabrication of ordered hydrophobic nanocone array decorated with hydrophilic spots SALDI substrate(C), the SEM in the cross?sectional view(D) and the detection reproducibility(E)[47](A, B) Copyright 2013, American Chemical Society; (C—E) Copyright 2018, Elsevier.
Fig.7 SEM(A) and SALDI?MS detection efficiency(signal intensity, S/N) (B) of Au nanoparticle grafted nanostructured silicon[50], schematic representation to the fabrication half hydrophilic and half hydrophobic Au nanoparticle assisted nanostructured silicon substrate(C) and MS imaging of fingerprints(D)[51], preparation schematic illustration(E), SEM(F) and detection sensitivity(G) of the super?hydrophobic Au coated silicon nanocone array[52](A, B) Copyright 2015, American Chemical Society; (C, D) Copyright 2020, American Chemical Society; (E—G) Copyright 2019, Elsevier.
Fig.8 Schematic diagram(A) and fingerprint MS imaging(B) on Ag coating nanostructured silicon[53], pre-paration schematic illustration(C), detection sensitivity(D) and detection reproducibility(E) of silicon pillar with hydrophilic top and hydrophobic bottom and side walls recombination with Ag nanoparticle[55](A, B) Copyright 2015, American Chemical Society; (C—E) Copyright 2019, Springer Nature.
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