1 | 1.33—1.36(m, 2H), 1.39(s, 9H), 1.41—1.43(m, 2H), 1.74(s, 2H), 2.00(t, 2H), 2.54(s, 2H), 2.86—2.89(m, 4H), 2.99—3.00(m, 2H), 4.28(t, 1H), 4.48—4.49(m, 2H), 6.64(d, 2H,J=7.5 Hz), 7.66(d, 2H, J=8.6 Hz), 8.64(s, 1H) | |
2 | 1.38(m, 4H), 1.50(m, 4H), 1.74(m, 2H), 2.06(m, 2H), 2.76(m, 2H), 3.02(m, 2H), 4.30(m, 1H), 4.50(s, 2H), 6.64(d, 2H, J=8.3 Hz), 7.66(d, 2H, J=8.4 Hz), 8.66(s, 1H) | |
3* | 1.45(s, 9H), 2.85(s, 4H), 3.88(d, 2H), 4.43(d, 2H) | |
4 | 1.37(s, 9H), 1.74(m, 2H), 2.54(m, 4H), 3.03—3.04(m, 2H), 3.55(d, 2H), 3.64(d, 2H), 4.24—4.30(m, 1H), 4.48(d, 2H), 6.64(d, 2H, J=8.7 Hz), 7.66(d, 2H, J=8.7 Hz), 8.65(s, 1H) | |
5 | 1.21(m, 2H), 1.31(m, 2H), 1.64(m, 2H), 4.09(m, 5H), 4.41(m 6H), 6.58(d, 2H), 7.58(d, 2H), 8.57(s, 1H) | |
6 | 1.38(m, 3H), 1.49(m, 2H), 1.75(m, 2H), 1.90(m, 1H), 2.06(m, 1H), 2.50(m, 3H), 2.74(m, 1H), 2.93(m, 6H), 3.21(m, 3H), 4.29(s, 1H), 4.49(s, 2H), 6.65(d, 2H), 6.92(m, 3H), 7.49(s, 1H), 7.67(m, 3H), 8.04(m, 2H), 8.65(m, 2H) | 20.99, 22.89, 23.25, 28.75, 28.88, 30.37, 35.12, 38.18, 45.91, 52.38, 104.74, 111.17, 111.91, 120.32, 121.41, 127.46, 127.88, 128.94, 131.10, 136.76, 141.81, 148.52, 150.70, 153.81, 158.45, 161.07, 164.83, 166.37, 167.36, 171.97, 174.19 |
7 | 1.34(m, 4H), 1.72(m, 2H), 2.71(m, 2H), 2.93(m, 4H), 3.03(m, 2H), 3.84(m, 3H), 4.24(m, 2H), 4.46(s, 2H), 6.62(d, 2H), 6.94(m, 3H), 7.65(m, 3H), 8.04(m, 3H), 8.63(m, 2H) | 23.19, 28.67, 30.46, 38.35, 40.41, 42.06, 42.86, 45.91, 52.43, 104.76, 111.71, 177.78, 119.60, 121.47, 122.51, 127.51, 128.93, 131.07, 136.94, 142.03, 147.91, 148.51, 150.70, 151.91, 153.85, 156.21, 160.81, 165.61, 166.33, 167.34, 168.49, 169.44 |