Chem. J. Chinese Universities ›› 1985, Vol. 6 ›› Issue (1): 69.
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Pan Zuohua1, Jin Xianlin1, Shao Meicheng1, Zhuang Ruifang2, Xiao Yongzhuang2
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Abstract: This thesis reports crystal structure of the complex, K4Na3{Cu[C-(CH)5(OH)(PO5)2]2}·12H2O. The structure was determined by Patterson method and refined by block least squares routine.The final deviation factor is:R= 0.0413.Title compound crystallizes in space group P1 with crystall-ographic parameters a=ll.951(3), b = 6.220(1), c = 11. 789(2)Å; α=113.166 (11)°β= 108.944(15)° γ = 97.563(14)°;V = 727.4Å5; Dc = 2.02g/cmÅ3 and μ(MoKa) = 16.9cm-1.The result of crystal structure, analysis shows that the copper atom in each chelate ion is coordinated by four oxygen atoms of phosphoryt groups and two oxygen atoms of hydroxyl groups.
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Pan Zuohua, Jin Xianlin, Shao Meicheng, Zhuang Ruifang, Xiao Yongzhuang. Crystal Structure Research of Complex K4Na2{Cu[C(CH3)(OH)(PO3)2]2}·12H2O[J]. Chem. J. Chinese Universities, 1985, 6(1): 69.
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