Chem. J. Chinese Universities ›› 1999, Vol. 20 ›› Issue (12): 1897.
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LI Run-Tao, GE Ze-Mei, CHENG Tie-Ming, CAI Meng-Shen
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Abstract: In the presence of anhydrous potassium phosphate, different kinds of dithiocarbamates were prepared from the reaction of primary amines, secondary amines and piperazine with carbon disulfate and a variety of alkyl halides at room temperature in high yields. It is not affected for the presence of -CONR 2, -OH, -CO2H,-NO2, -CO2R, -CH(OR)2, -C=C-, -CH2OR, furan ring and saccharide ring in amine or alkyl halide.
Key words: Anhydrous potassium phosphate, Dithiocarbamate, New synthetic method
CLC Number:
O624
TrendMD:
LI Run-Tao, GE Ze-Mei, CHENG Tie-Ming, CAI Meng-Shen . New Synthetic Method for Dithiocarbamates[J]. Chem. J. Chinese Universities, 1999, 20(12): 1897.
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http://www.cjcu.jlu.edu.cn/EN/Y1999/V20/I12/1897
