The Synthesis and Characterization of Epoxy-terminated Phenolphthalein Poly(cyanoarylether)

Chem. J. Chinese Universities ›› 1998, Vol. 19 ›› Issue (4): 661.

• Articles • Previous Articles Next Articles

The Synthesis and Characterization of Epoxy-terminated Phenolphthalein Poly(cyanoarylether)

LIAO Wei-Lin, ZENG Xiao-Jun, CUI Guo-Di, WANG Sheng

Department of Chemistry, Jiangxi Normal University, Nanchang, 330027

Received:1996-12-14 Online:1998-04-24 Published:1998-04-24

Abstract

Abstract: Epoxy-terminated poly(cyanoarylether)(E-PCE) with M_n from 1000 to 12000 were synthesized by the reaction of epichlorohydrin with PCEoligomer with —OK terminal groups prepared by condensation of phenolphthalein (PPH) with 2,6-dichlorobenzonitrile (DCBN) using K₂CO₃ as catalyst. The E-PCEs were characterized by IR and ¹H NMR spectra, the solubility of E-PCE samples was also measured. In addition, the solidification action and the heat resisting quality of the fully crosslinked E-PCE/DDS were also measured by DSCand TGA.

Key words: Epoxy-terminated, Poly(cyanoarylether), Synthesis and characterization

CLC Number:

O631

TrendMD:

LIAO Wei-Lin, ZENG Xiao-Jun, CUI Guo-Di, WANG Sheng . The Synthesis and Characterization of Epoxy-terminated Phenolphthalein Poly(cyanoarylether)[J]. Chem. J. Chinese Universities, 1998, 19(4): 661.

[1]	LUO Yong-Ming^1,2, HOU Zhao-Yin¹, ZHENG Xiao-Ming¹*. Synthesis and Characterization of Ordered Mesoporous Aluminosilicates Molecular Sieves with Highly Hydrothermal Stability [J]. Chem. J. Chinese Universities, 2007, 28(5): 801.
[2]	XU Ning, WU Tong-Hao, WANG Dong-Yang, WU Peng, KAN Qiu-Bin, SUN Jia-Zhong . Synthesis and Characterization of a Novel Layered Zeolite MCM-56 [J]. Chem. J. Chinese Universities, 2001, 22(11): 1898.
[3]	SHAN Yong-Kui, XIE Wen-Hua, YE Xing-Kai, WU Yue. Synthesis,Characterization and Catalytic Activity for H₂O₂ Decomposition of Tetrabasic Tugstovanadophosphate Heteropoly Rare Earth Element Complexes with Dawson Structure [J]. Chem. J. Chinese Universities, 1996, 17(4): 613.
[4]	ZHANG Fu-Shun, WU Zhi-Yun, ZHANG Chun-Lei, KAN Qiu-Bin . Studies on the Synthesis and Characterization of Ti-ZSM-11 and the Selective Oxidation of Styrene [J]. Chem. J. Chinese Universities, 1995, 16(4): 603.
[5]	GUO Jun, SUN Tie, SHEN Jian-Ping, LIU Dan, DANG Da-Zhen, MIN En-Ze. Synthesis, Characterization and Acid-Base Properties of Layered Double Hydroxides Pillared with Tungstosilicate Anions [J]. Chem. J. Chinese Universities, 1995, 16(3): 346.
[6]	WANG Yong-Wei, ZHANG Hua-Lin. Synthesis and Characterization of N,N'-Bis(2-hydroxybenzylidene)-2-hydroxyphenymethanediamine and N,N'-Bis-(2-hydroxybenzyl)-2-hydroxyphenylmethanediamine complexes with transition metals [J]. Chem. J. Chinese Universities, 1994, 15(6): 794.

The Synthesis and Characterization of Epoxy-terminated Phenolphthalein Poly(cyanoarylether)

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 6

Recommended Articles

Metrics

Comments