Isolation and X-ray Crystallographic Stucture of Cyclic Tetramer Based on Bisphenol A and o-Phthaloyl Dichloride

Chem. J. Chinese Universities ›› 1996, Vol. 17 ›› Issue (8): 1310.

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Isolation and X-ray Crystallographic Stucture of Cyclic Tetramer Based on Bisphenol A and o-Phthaloyl Dichloride

JIANG Hong-Yan, LIU Tian-Xi, CHEN Tian-Lu, MO Zhi-Shen, XU Ji-ping

Changchun Institute of Applied Chemistry, Academia Sinica, Changchun 130022

Received:1995-07-31 Online:1996-08-24 Published:1996-08-24

Abstract

Abstract: The polycrystalline powder of the cyclic tetramer based on bisphenol Aand o-phthaloyldichloride has been prepared by recrystallization from nitrobenzene and its crystalstructure has been determined by Wide-Angle X-ray Diffraction( WAXD ).The unit cell is orthorhombic and its dimensions α=0.967 b=0.8699 nm,c=2.0859 nm.Space group belongs to Pmmm,With two tetramers per unit cell, the crystal density is 1.36 g·cm^-3.Indices of crystal diffraction peaks are also detailed in the present work.

Key words: Cyclic tetramer, WAXD, Unit cell parameter

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JIANG Hong-Yan, LIU Tian-Xi, CHEN Tian-Lu, MO Zhi-Shen, XU Ji-ping. Isolation and X-ray Crystallographic Stucture of Cyclic Tetramer Based on Bisphenol A and o-Phthaloyl Dichloride[J]. Chem. J. Chinese Universities, 1996, 17(8): 1310.

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Isolation and X-ray Crystallographic Stucture of Cyclic Tetramer Based on Bisphenol A and o-Phthaloyl Dichloride

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