Chem. J. Chinese Universities ›› 1994, Vol. 15 ›› Issue (5): 708.
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SHA Yao-Wu, CAI Meng-Shen
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Abstract: Cyanogen hydrazide reacted with triethyl orthoformate at 140℃for 24 h.Through column separation,two compounds 1-(ethoxymethyleneiminyl)imidazolo-(5,4-e)-1,2,4-triazine and 5-methoxy-6-ethylamino 1,2,4-triazine were obtained.If the cyanogen hydrazide reacted with triethyl orthoformate at 100℃ for 24h,another compound.1-ethylamino-imidazolo(5,4-e)-1,2,4-triazine was obtained.
Key words: Cyanogen hydrazide, Triethyl orthoformate, 1,2,4-Triazine, Imidazolo-(5,4-e)-1,2,4-triazine
TrendMD:
SHA Yao-Wu, CAI Meng-Shen . Chemistry of 1,2,4-Triazines(XXII)──Synthesis of Imidazolo-(5,4e)-1,2,4-triazine[J]. Chem. J. Chinese Universities, 1994, 15(5): 708.
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http://www.cjcu.jlu.edu.cn/EN/Y1994/V15/I5/708