Chem. J. Chinese Universities ›› 1992, Vol. 13 ›› Issue (8): 1063.
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YANG Hua-Zheng, ZHANG Yue-Hua
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Abstract: Using THF as the solvent,a series of new 2-substituted phenoxyl(anilino)-1,3,2-ox-azaphospholidine derivatives were prepared by the reaction of phosphorus sulfochloride with ami-noethanol directly and then treating with phenol or aniline in the presence of triethylamine.This is one pot reaction without the separation and purification of any intermediate and a high yield was obtained.AHof these compounds were confirmed by 1H NMR,IR,MS and elementary analysis,Their 1H NMR,and MS spectra and biological activity are discussed.
Key words: 1,3,2-Oxazaphosphoiidine, Phosphorus sulfochloride, β-Hydroxyethylamine
TrendMD:
YANG Hua-Zheng, ZHANG Yue-Hua . 1,3,2-Oxazaphospholidine Derivatives(Ⅲ)——Studies on Synthesis and Biological Activity of 1,3,2-OxazaphosphoIidine Derivatives[J]. Chem. J. Chinese Universities, 1992, 13(8): 1063.
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http://www.cjcu.jlu.edu.cn/EN/Y1992/V13/I8/1063
