Chem. J. Chinese Universities ›› 1987, Vol. 8 ›› Issue (7): 629.
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Lin Xiuyun. Zheng Qitai1, Wu Shen1, Zhang Shude1, Shen Fuling1, Wang Jitao1, Xie Qinglan2, Liao Renan2, Li Jing2
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Abstract: Silatrane Ibelongs to monoclinic system with space group P21/N(Z=4) and silatrane Ⅱ belongs to orthorhombic system with space group Pcab(Z= 8).The lattice parameters are.Ⅰ,α= 11.876(2)Å, 6=19.853(4)Å, c= 6.598(1)Å, β=110.12(2) Ⅱ.α= 19.653(4)Å, b=12.565(3)Å, c=12.570(3)Å.The structures were solved by RANTAN and refined by Full Matrix Least-Square Method. The final R-factors are 0.09 and 0.06, respectively.The N→Si bond of silatrane Iis shorter than that of Iand both of them are shorter than those of other kinds of silatranes.
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Lin Xiuyun. Zheng Qitai, Wu Shen, Zhang Shude, Shen Fuling, Wang Jitao, Xie Qinglan, Liao Renan, Li Jing. Study of the Crystal Structures of Silatranes (这里有图片198707-634-1.gif)[J]. Chem. J. Chinese Universities, 1987, 8(7): 629.
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