CJCU

Chem. J. Chinese Universities ›› 1986, Vol. 7 ›› Issue (11): 1031.

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Crystal and Molecular Structure of C5H5FeC6H4SO2N （C2H4CN）CH2C6H5

Xin Min1, Han Yuding1, Liu Qiwang1, Hu Yucai1, Huang Jinsun2   

  1. 1. Neimenggu University Huhehaote;
    2. Fujian Institute oj Research of the Structure of Matter, Academia Sinica Fuzhou
  • Received:1985-07-30 Online:1986-11-24 Published:1986-11-24

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Abstract: The crystal structure of C5H5FeC5H4SO2N(C2H4CN)CH2C6H5 was determined by X-ray analysis The crystal is monoclinic,belonging to space group P21/n with unit cell dimensions.a=8.750(1),b=12.876(5),c=16.744(2)Å β=94.75(1),V=1880.0Å3,Z=4,Dc=1.442g/cm3.The intensities of 2226 independent reflections with I≥2°(I)were collected on a GAD-4 four-circle diffractometer using Mo Ka radiation.The structure was solved by Patterson method and difference fourier synthesis,and refined by full-matrix Least-squares.Final discrepancy factor R=0.0466.All calculations were performed with a PDP 11/34 computer using SDPprograms.The coordination features of Sand Natoms of the molecule are discussed.The crystal structure of C5H5FeC5H4SO2N(C2H4CN)CH2C6H5 was determined by X-ray analysis The crystal is monoclinic,belonging to space group P21/n with unit cell dimensions.a=8.750(1),b=12.876(5),c=16.744(2)A β=94.75(1),V=1880.0A3,Z=4,Dc=1.442g/cm3.The intensities of 2226 independent reflections with I≥2°(I)were collected on a GAD-4 four-circle diffractometer using Mo Ka radiation.The structure was solved by Patterson method and difference fourier synthesis,and refined by full-matrix Least-squares.Final discrepancy factor R=0.0466.All calculations were performed with a PDP11/34 computer using SDPprograms.The coordination features of Sand Natoms of the molecule are discussed.

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