CJCU

Chem. J. Chinese Universities ›› 1985, Vol. 6 ›› Issue (3): 238.

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Analysis of Organometallic Compounds (v)——A Study on the Paper Chromatography and Nuclear Magnetic Resonance of Bis(Alkylpentadienyl)Titanium, Zirconium and Hafnium Dihalides

Yang Xuejin1, Li Songlan1, Chen Shoushan2, Liu Yiyin2   

  1. 1. Department of Chemistry, Nankai University, Tianjin;
    2. Institute of Elemento-Orgenic Chemistry, Nankai University, Tianjin
  • Received:1983-09-02 Online:1985-03-24 Published:1985-03-24

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Abstract: Paper chromatography and nuclear magnetic resonance for bis(alkylpcntadienyl)-titanium, zirconium and hafnium dihalides have been studied.Decane-heptane-acetone (1:5:6) and decane-cyclohexane-acetonc (1:5:6) solvent systems were used for the separation of bis(alkylpentadienyl)titanium, zirconium and hafnium dihalides by paper chromatography.The results have been discussed based on the relation among the obtained R1, δ values and other molecular characteristics.

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