CJCU

Chem. J. Chinese Universities ›› 1984, Vol. 5 ›› Issue (2): 276.

• Articles • Previous Articles     Next Articles

STUDIES ON THE SYNTHESIS, STRUCTURE AND PROPERTIES OF THE CRYSTAL OF Mo-Fe-S COMPLEX

Zhang Zhigui1, Wang Fengshan1, Li Shuqin1, Zhao Chengzhi2, Li Ying2   

  1. 1. Department of Chemistry, Jilin University, Changchun;
    2. Institute of Theoretical Chemistry, Jilin University, Changchun
  • Received:1982-10-06 Online:1984-04-24 Published:1984-04-24

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Abstract: In this paper, we report a new complex of Mo-Fe-Ssynthesized by the reaction of MoCl5, FeCl2·4H2O, PhCH2SH and diethyldithiocarba-mate(DTC) in MeOH, The complex is characterized by X-ray crystal-lography,IR,UV-visible, 1H NMR, 13C NMR, and EPRspectra, and the measurements of elemental analyses and electrochemical properties. The crystal of Mo-Fe-Scomplex containing multi-bond species is quite stable.

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