Chem. J. Chinese Universities ›› 2019, Vol. 40 ›› Issue (4): 832.doi: 10.7503/cjcu20180685
• Polymer Chemistry • Previous Articles Next Articles
CAI Lihai, GUO Baohua*(), ZHANG Cheng, XU Jun, HUANG Zhongyao
Received:
2018-10-10
Online:
2019-04-03
Published:
2019-04-10
Contact:
GUO Baohua
E-mail:bhguo@mail.tsinghua.edu.cn
Supported by:
CLC Number:
TrendMD:
CAI Lihai,GUO Baohua,ZHANG Cheng,XU Jun,HUANG Zhongyao. Long-term Stress Relaxation Prediction for Nylon 1010 Using Time-temperature Superposition Method†[J]. Chem. J. Chinese Universities, 2019, 40(4): 832.
Fig.1 Relaxation modulus of relaxation samples under different initial strains(A) 1.0% strain; (B) 2.8% strain; (C) 5.1% strain. 293 K; 303 K; 313 K; 323 K; 333 K; 343 K; 353 K.
Fig.4 Azimuthal X-ray diffraction intensity curves of Nylon 1010 samples(A) (002) reflection; (B) (100) reflection. a. Initial; b. 5.1% strain at 293 K; c. 5.1% strain at 313 K; d. 5.1% strain at 353 K.
Sample | ΔH/(J×g-1) | Xc(%) | Π(%) |
---|---|---|---|
Initial | 93.6 | 38.4 | 51.2 |
5.1% strain at 293 K | 94.8 | 38.9 | 50.5 |
5.1% strain at 313 K | 93.5 | 38.3 | 52.2 |
5.1% strain at 333 K | 95.5 | 39.1 | |
5.1% strain at 353 K | 94.6 | 38.8 | 50.3 |
Table 1 Crystallinity(Xc) and orientation degree(Π) of Nylon 1010 samples
Sample | ΔH/(J×g-1) | Xc(%) | Π(%) |
---|---|---|---|
Initial | 93.6 | 38.4 | 51.2 |
5.1% strain at 293 K | 94.8 | 38.9 | 50.5 |
5.1% strain at 313 K | 93.5 | 38.3 | 52.2 |
5.1% strain at 333 K | 95.5 | 39.1 | |
5.1% strain at 353 K | 94.6 | 38.8 | 50.3 |
Initial strain(%) | ΔHa/(kJ×mol-1) | Temperature/K |
---|---|---|
1.0 | 596 | 293—323 |
263 | 333—353 | |
2.8 | 432 | 293—323 |
259 | 333—353 | |
5.1 | 356 | 293—323 |
258 | 333—353 |
Table 2 Apparent activation energies(ΔHa) in Arrhenius plots of Fig.6
Initial strain(%) | ΔHa/(kJ×mol-1) | Temperature/K |
---|---|---|
1.0 | 596 | 293—323 |
263 | 333—353 | |
2.8 | 432 | 293—323 |
259 | 333—353 | |
5.1 | 356 | 293—323 |
258 | 333—353 |
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