高等学校化学学报

高等学校化学学报 ›› 1999, Vol. 20 ›› Issue (S1): 252.

• Chromatography and Separation Sciences • 上一篇    下一篇

Preparation and Evaluation of Calix[8]arene Bonded Silica Stationary Phase for High Performance Liquid Chromatography

XIAO Xiang-Zhu1, FENG Yu-Qi1, DA Shi-Lu1, ZHANG Yan2   

  1. 1. Department of Chemistry, Wuhan University 430072, P. R. China;
    2. Laboratory of MRAMP of China, Wahan 430072, P. R. China
  • 出版日期:1999-12-31 发布日期:1999-12-31

Preparation and Evaluation of Calix[8]arene Bonded Silica Stationary Phase for High Performance Liquid Chromatography

XIAO Xiang-Zhu1, FENG Yu-Qi1, DA Shi-Lu1, ZHANG Yan2   

  1. 1. Department of Chemistry, Wuhan University 430072, P. R. China;
    2. Laboratory of MRAMP of China, Wahan 430072, P. R. China
  • Online:1999-12-31 Published:1999-12-31

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摘要：

In recent years, calix[n]arenes (n=4,5,6,7,8) as stationary phase have been introduced into the field of chromatography. In our previous works, we have synthesized, characterized and evaluated two different silica-bonded calix[n]arenes (n=4,6) stationary phase, on which the chromatographic behavior of PAHs, positional isomers,nucleosides and bases was investigated. In this paper we report the preparation of calix[8]arene bonded silica stationary phase, and characterization of its structure and chromatographic behavior.

Abstract:

In recent years, calix[n]arenes (n=4,5,6,7,8) as stationary phase have been introduced into the field of chromatography. In our previous works, we have synthesized, characterized and evaluated two different silica-bonded calix[n]arenes (n=4,6) stationary phase, on which the chromatographic behavior of PAHs, positional isomers,nucleosides and bases was investigated. In this paper we report the preparation of calix[8]arene bonded silica stationary phase, and characterization of its structure and chromatographic behavior.

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