高等学校化学学报 ›› 2000, Vol. 21 ›› Issue (S1): 414.

• Chemistry in Surface Science • 上一篇    下一篇

A Rapid Method of Measurement Hydrogen Chemisorption on Supported Metal Catalyst

ZHU Yi-Feng, LI Xiao-Nian   

  1. Institute of Catalysis, Zhejiang University of Technology, Hangzhou 310014
  • 出版日期:2000-12-31 发布日期:2000-12-31
  • 基金资助:

    This project was financially supported by Provincial Natural Science Foundation of Zhejiang (299015) and the development plan of youth mainstay teacher of the Education Ministry of China.

A Rapid Method of Measurement Hydrogen Chemisorption on Supported Metal Catalyst

ZHU Yi-Feng, LI Xiao-Nian   

  1. Institute of Catalysis, Zhejiang University of Technology, Hangzhou 310014
  • Online:2000-12-31 Published:2000-12-31
  • Supported by:

    This project was financially supported by Provincial Natural Science Foundation of Zhejiang (299015) and the development plan of youth mainstay teacher of the Education Ministry of China.

摘要:

The surface area and dispersion of a supported metal catalyst can be conveniently determined form the measurement of a chemisorbed monolayer of an appropriate adsorbate such as hydrogen at conditions under which little or no adsorption occurs on the support. Such measurements can be carried out by means of conventional high-vacuum-adsorption apparatus[1],but more rapid flow methods of measuring chemisorption are often found useful[2]. This is especially true when the need arises to characterize the multitude of catalyst samples generated by varying preparation, support, pretreatment and use of a given series of supported metals.

Abstract:

The surface area and dispersion of a supported metal catalyst can be conveniently determined form the measurement of a chemisorbed monolayer of an appropriate adsorbate such as hydrogen at conditions under which little or no adsorption occurs on the support. Such measurements can be carried out by means of conventional high-vacuum-adsorption apparatus[1],but more rapid flow methods of measuring chemisorption are often found useful[2]. This is especially true when the need arises to characterize the multitude of catalyst samples generated by varying preparation, support, pretreatment and use of a given series of supported metals.

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