高等学校化学学报

高等学校化学学报 ›› 1998, Vol. 19 ›› Issue (S1): 369.

• Organometallic Chemistry • 上一篇    下一篇

Study on'the α-Thiocarbonylthioformamide Ⅱ——Dehydrogenation of tetrahydronaphthalene

Run Sun Zeng, Jian Ping Zou, Zhong E Lu, Jian Feng Ge, Ke Qian Chen   

  1. Department of Chemistry, Suzhou University, Suzhou, 215006 Jiangsu
  • 出版日期:1998-12-31 发布日期:1998-12-31

Study on'the α-Thiocarbonylthioformamide Ⅱ——Dehydrogenation of tetrahydronaphthalene

Run Sun Zeng, Jian Ping Zou, Zhong E Lu, Jian Feng Ge, Ke Qian Chen   

  1. Department of Chemistry, Suzhou University, Suzhou, 215006 Jiangsu
  • Online:1998-12-31 Published:1998-12-31

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摘要： α-Thiocarbonylthioformamides were synthesized in 1980[1-3]. Authors first explored their dehydrogenation reaction at high temperature. In our initial experiment, α-Thiobenzoylthioformmorpholine(l) was heated with diethyl acetylene dicarboxylate in tetrahydronaphthalene(2). The reaction is shown as following.

Abstract: α-Thiocarbonylthioformamides were synthesized in 1980[1-3]. Authors first explored their dehydrogenation reaction at high temperature. In our initial experiment, α-Thiobenzoylthioformmorpholine(l) was heated with diethyl acetylene dicarboxylate in tetrahydronaphthalene(2). The reaction is shown as following.

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