Facile Preparation of Zeolitic Imidazole Frameworks by Thermal Treatment Solid-Phase Transformation

doi:10.7503/cjcu20200010

Abstract

Abstract: The facile synthesis of zeolitic imidazolate frameworks(H-ZIF-67) under fully avoided solvent and a short reaction was achieved. The solid-phase transformation of mixed metal and organic ligand sources during the heat treatment process was a crucial mechanism of synthesis strategy. The synthesized materials were characterized by means of powder-XRD, SEM, TEM, TGA, FTIR, porosity, and N₂ adsorption-desorption analyses. The results illustrate the characteristic properties compatibility with the commercial methods for the preparation of ZIF-67 have been reported. The single-step, truly solvent-free, non-post treatment, short-time synthesis, and safety system as ambient pressure, were an advantage of this developed method.

Key words: Zeolite imidazolate framework material, Solid phase transformation, Solvent-free synthesis, Heat treatment

CLC Number:

O614.8

TrendMD:

XU Wei, WANG Jichao, SHI Guangyong, CHAEMCHUEN Somboon. Facile Preparation of Zeolitic Imidazole Frameworks by Thermal Treatment Solid-Phase Transformation[J]. Chem. J. Chinese Universities, 2020, 41(8): 1753.

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