Study on the Technique of ICP-AES by Using Electrothermal Graphite Furnace as Sample Introduction Device——Device and Its Analytical Performance

Abstract

Abstract: An instrument system is described in which a graphite furnace electrothermal vaporization device is used for the.introduction of microlitre liquid sample into an inductively coupled plasma.The appratus is equipped with home-made ones.Under the optimum operating condition for ICPexcitation and graphite furnace evaporation, the detection limits are at sub-nanogram level with linear dynamic ranges of over four orders of magnitude for nine elements.The RSDare better than 5%.

Key words: Graphite furnace, Electrothermal vaporization, Inductively coupled plasma(ICP), Combined technique

TrendMD:

Huang Min, Xu Lianfa, Jiang Zucheng, Zeng Yun'e . Study on the Technique of ICP-AES by Using Electrothermal Graphite Furnace as Sample Introduction Device——Device and Its Analytical Performance[J]. Chem. J. Chinese Universities, 1989, 10(7): 709.

[1]	GUAN Hongyan, LIAN Fang, WEN Yan, PAN Xiaorong, SUN Jialin. Thermal Stability of Novel Polyvinyl Formal Based Gel Polymer Electrolyte^† [J]. Chem. J. Chinese Universities, 2014, 35(1): 80.
[2]	WU Ying-Liang, HU Bin, JIANG Zu-Cheng . Studies on the Chemical Modification and Its Mechanism of Acetylacetone in Low Temperature ETV-ICP-AES [J]. Chem. J. Chinese Universities, 2004, 25(1): 50.
[3]	HANG Yi-Ping, QIN Yong-Chao, JIANG Zu-Cheng, HU Bin . Direct Analysis of Trace Rare EartHElements Through Nanometer-size Titanium Dioxide Separation/Concentration and Fluorination Assisted ETV-ICP-AES with Slurry Sampling [J]. Chem. J. Chinese Universities, 2003, 24(11): 1980.
[4]	WU Ying-Liang, JIANG Zu-Cheng, HU Bin . A Novel Micro Drop Solvent Extraction Technique Combined with Low Temperature Electrothermal Vaporization ICP-AES for Ultra Trace Element Analysis [J]. Chem. J. Chinese Universities, 2003, 24(10): 1793.
[5]	XIONG Hong-Chun, HU Bin, JIANG Zu-Cheng . A Miniaturization Solid-phase Extraction Technique Designed for Electrothermal Vaporization-Atomic Emission Spectrometry Determination [J]. Chem. J. Chinese Universities, 2000, 21(7): 1035.
[6]	PENG Tian-You, YAN Qin, HU Bin, JIANG Zu-Cheng . Direct Determination of Trace Impurity Yttrium in Titantium Oxide Powder by Fluorination Assisted ETV-ICP-AES Using Slurry Sampling [J]. Chem. J. Chinese Universities, 2000, 21(5): 694.
[7]	XIONG Hong-Chun, HU Bin, HUANG Wei-Hong, PENG Tian-You, CHEN Shi-Zhong, JIANG Zu-Cheng . Determination of Trace Amounts of Rare Earth Elements by ETV-ICP-AES Combined with Microcolumn Separation/Preconcentration [J]. Chem. J. Chinese Universities, 2000, 21(11): 1647.
[8]	SU Xing-Guang, ZHANG Han-Qi, LIANG Feng, JIN Qin-Han, BAI Suo-Zhu . Studies on the On-line Anion Exchange Preconcentration for Graphite Furnace Atomic Absorption Spectrometry [J]. Chem. J. Chinese Universities, 1999, 20(8): 1189.
[9]	PENG Tian-You, JIANG Zu-Cheng  . Determination of Scandium in ETV-ICP-AES by Using PMBP as Chemical Modifier [J]. Chem. J. Chinese Universities, 1998, 19(5): 699.
[10]	HE Zhi-Rong, CHEN Jiang-Han, HE Hua-Kun . A Study on Analytical Performance of THGF [J]. Chem. J. Chinese Universities, 1998, 19(4): 534.
[11]	TANG You-Wen, SONG Jian-Yi, MO Sheng-Jun. Preconcentration of Silver on Blue Algae Determination by Slurry Graphite Furnace Atomic Absorption Spectrometry [J]. Chem. J. Chinese Universities, 1995, 16(12): 1865.
[12]	ZHUANG Zhi-Xia, YANG Peng-Yuan, WANG Xiao-Ru, XUE Ru, HUANG Ben-Li. A Study of Glassy Carbon Material as Platform with Graphite Furnace Atomic Absorption Spectrometry [J]. Chem. J. Chinese Universities, 1994, 15(9): 1297.
[13]	ZHENG Yan-Sheng, SU Xing-Guang, QUAN Zhe. Study on Factors Influencing Characteristic Mass in Graphite Furnace Atomic Absorption Spectrometry [J]. Chem. J. Chinese Universities, 1993, 14(7): 937.
[14]	HU Bin, JIANG Zu-Cheng, ZENG Yun-E. The Study on Vaporization Mechanisms of Vanadium and Titanium in ICP-AES with Sample Introduction by Graphite Furnace Electrothermal Vaporization [J]. Chem. J. Chinese Universities, 1993, 14(12): 1665.
[15]	YU Ai-Min, ZHANG Han-Qi, LIU Xiao-Jing, JIN Qin-Han . Studies on Determination of Copper, Zinc, Cadmium by Electrothermal Vaporization Feeding and Low Powered MPT-AES [J]. Chem. J. Chinese Universities, 1993, 14(1): 44.

Study on the Technique of ICP-AES by Using Electrothermal Graphite Furnace as Sample Introduction Device——Device and Its Analytical Performance

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments