3A | 9.44—9.36(m, 2H), 9.25(t, J=5.7 Hz, 2H), 8.33(d, J=7.9 Hz, 2H), 7.70(t, J=7.7 Hz, 2H), 7.50(d, J=8.4 Hz, 2H), 7.43(t, J=7.5 Hz, 2H), 7.30(t, J=7.6 Hz, 2H), 7.19(d, J=7.7 Hz, 4H), 3.54—3.47(m, 6H), 1.19(d, J=6.7 Hz, 12H) | 164.42, 146.14, 143.18, 138.73, 138.45, 137.44, 131.55, 131.44, 129.53, 128.17, 123.44, 122.25, 121.54, 121.19, 115.37, 109.83, 77.24, 77.03, 76.82, 32.39, 29.01, 23.78, 23.60 |
3B | 9.13(s, 2H), 8.36(s, 2H), 7.91(s, 2H), 7.68(s, 2H), 7.47(s, 2H), 7.43(t, J=7.5 Hz, 2H), 4.02(s, 2H), 3.31(s, 6H), 2.02(s, 4H), 1.69(s, 4H), 1.61(d, J=13.1 Hz, 2H), 1.44—1.37(m, 4H), 1.21(s, 4H), 1.12(d, J=30.4 Hz, 2H) | 164.11, 143.00, 139.05, 138.35, 137.13, 131.07, 129.23, 122.16, 121.50, 120.87, 114.72, 109.89, 48.38, 33.30, 32.28, 25.55, 25.08 |
3C | 9.14(s, 2H), 8.35(d, J=7.9 Hz, 2H), 7.94(d, J=8.0 Hz, 2H), 7.68(t, J=7.7 Hz, 2H), 7.46(d, J=8.3 Hz, 2H), 7.43(t, J=7.5 Hz, 2H), 4.49—4.43(m, 2H), 3.29(s, 6H), 2.07(dt, J=13.0, 5.6 Hz, 4H), 1.68—1.63(m, 4H), 1.63—1.57(m, 4H), 1.48(dt, J=12.4, 6.2 Hz, 4H) | 164.70, 142.99, 138.99, 138.38, 137.13, 131.01, 129.26, 122.15, 121.49, 120.90, 114.69, 109.90, 51.18, 33.26, 32.22, 23.87 |
3D | 9.12(s, 2H), 8.32(d, J=7.9 Hz, 2H), 7.95(s, 2H), 7.68(t, J=7.6 Hz, 2H), 7.46(d, J=8.3 Hz, 2H), 7.41(t, J=7.5 Hz, 2H), 3.28(d, J=8.8 Hz, 6H), 1.47(s, 18H) | 164.42, 143.00, 139.71, 138.19, 137.11, 131.07, 129.22, 122.08, 121.50, 120.85, 114.23, 109.87, 51.00, 32.18, 28.97 |
3E | 9.14(s, 2H), 8.35(d, J=7.9 Hz, 2H), 7.85(d, J=8.3 Hz, 2H), 7.68(t, J=7.7 Hz, 2H), 7.47(d, J=8.3 Hz, 2H), 7.43(t, J=7.5 Hz, 2H), 4.35(dq, J=13.4, 6.6 Hz, 2H), 3.29(d, J=8.7 Hz, 6H), 1.24(t, J=6.1 Hz, 12H) | 164.25, 142.98, 139.00, 138.37, 137.13, 131.00, 129.26, 122.15, 121.47, 120.90, 114.71, 109.90, 41.45, 32.18, 22.81 |
4A | 12.68(s, 2H), 9.45(d, J=1.0 Hz, 2H), 8.25(d, J=7.9 Hz, 2H), 7.66(t, J=7.8 Hz, 2H), 7.45(dd, J=12.1, 6.4 Hz, 4H), 7.13—7.08(m, 6H), 3.40(d, J=0.6 Hz, 6H), 2.31(s, 12H) | 158.85, 143.93, 138.89, 134.79, 134.05, 132.99, 129.68, 129.32, 128.09, 127.02, 125.24, 122.96, 122.33, 121.86, 121.40, 109.97, 29.31, 18.83 |
4B | 11.07(d, J=7.8 Hz, 2H), 9.34(s, 2H), 8.22(d, J=7.9 Hz, 2H), 7.64—7.59(m, 2H), 7.42(t, J=7.5 Hz, 2H), 7.38(d, J=8.3 Hz, 2H), 4.08—4.00(m, 2H), 3.25(s, 6H), 2.02(dd, J=16.6, 13.2 Hz, 4H), 1.72(dd, J=13.1, 9.5 Hz, 6H), 1.60(dd, J=9.3, 3.9 Hz, 2H), 1.40(dd, J=18.5, 5.6 Hz, 4H), 1.22—1.11(m, 4H) | 159.61, 143.85, 138.52, 133.19, 129.05, 125.25, 122.63, 122.04, 121.73, 121.39, 120.89, 109.83, 48.92, 32.89, 29.48, 25.64, 24.89 |
4C | 11.03(t, J=14.7 Hz, 2H), 9.27(s, 2H), 8.14(d, J=7.9 Hz, 2H), 7.54(t, J=7.7 Hz, 2H), 7.34(t, J=7.5 Hz, 2H), 7.30(d, J=8.3 Hz, 2H), 4.37(dd, J=13.7, 6.9 Hz, 2H), 3.17(s, 6H), 2.00(dd, J=11.6, 4.9 Hz, 4H), 1.62(d, J=3.1 Hz, 4H), 1.51(dd, J=24.0, 13.2 Hz, 8H) | 159.12, 142.85, 137.51, 132.11, 128.06, 124.21, 121.64, 121.05, 120.70, 120.39, 119.83, 108.82, 50.58, 31.95, 28.50, 23.00 |
4D | 11.14(s, 2H), 9.36(d, J=1.0 Hz, 2H), 8.19(d, J=7.9 Hz, 2H), 7.63(t, J=7.7 Hz, 2H), 7.43(t, J=7.5 Hz, 2H), 7.39(d, J=8.2 Hz, 2H), 3.25(d, J=0.5 Hz, 6H), 1.51(s, 18H) | 159.38, 143.85, 138.51, 133.80, 129.01, 125.22, 122.63, 122.02, 121.60, 121.40, 120.51, 109.81, 51.49, 29.51, 28.77 |
4E | 11.00(d, J=7.5 Hz, 2H), 9.35(s, 2H), 8.21(d, J=7.9 Hz, 2H), 7.61(dd, J=11.4, 4.1 Hz, 2H), 7.42(t, J=7.5 Hz, 2H), 7.37(d, J=8.3 Hz, 2H), 4.33(dd, J=13.8, 6.7 Hz, 2H), 3.24(s, 6H), 1.27(dd, J=6.6, 3.2 Hz, 12H) | 159.69, 143.87, 138.51, 133.17, 129.10, 125.23, 122.68, 122.09, 121.71, 121.39, 120.88, 109.83, 41.99, 29.54, 22.61 |