Preparation and Magnetic Performance of Fe3O4/TiO2 Hybrid Nanostructure†

doi:10.7503/cjcu20140114

Abstract

Abstract:

Using TiO₂ nanowires and Fe(NO₃)₃·9H₂O as raw materials, Fe₃O₄ nanoparticles/TiO₂ nanowires hybrid nanostructure was fabricated in a system with diethylene glycol as the solvent. High-resolution transmission electron microscopy(HRTEM) observation demonstrates that the Fe₃O₄ nanoparticles are addressed on the TiO₂ nanowires. Effective connection forms between the Fe₃O₄ nanoparticles and TiO₂ nanowires. Magnetic study shows that the hybrid nanostructure’s blocking temperature is significantly lower than that of pure Fe₃O₄ nanoparticles with the same diameters.

Key words: Nanomaterial, Hybrid nanostructure, Magnetic property, Blocking temperature

CLC Number:

O611.4

TrendMD:

XU Man, DUAN Weijie, JIAO Shihui, PANG Guangsheng. Preparation and Magnetic Performance of Fe₃O₄/TiO₂Hybrid Nanostructure^†[J]. Chem. J. Chinese Universities, 2014, 35(5): 917.

Figures/Tables 4

Fig.1 XRD patterns of Fe3O4 nanoparticles(a) and Fe3O4 nanoparticles/TiO2 nanowires hybrid structure(b)

Fig.2 XPS spectrum of Fe3O4 nanoparticles

Fig.3 SEM(A), HRTEM(B) images of Fe3O4 nanoparticles/TiO2 nanowires hybrid structure and the lattice fringes of Fe3O4 nanoparticles and TiO2 nanowires(C)

Fig.4 Temperature dependence of ZFC and FC magnetization for Fe3O4 nanoparticles/TiO2 nanowires hybrid structure(A) and Fe3O4 nanoparticles(B) and magnetic hysteresis curves of the hybrid structure(C)

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Preparation and Magnetic Performance of Fe₃O₄/TiO₂Hybrid Nanostructure^†

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